Title:
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Flowback of solids through distribution plates of gas fluidized beds and associated phenomena
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This work is concerned with a study of certain phenomena related to
the performance and design of distributors in gas fluidized beds with
particular regard to flowback of solid particles. The work to be described
is divided into two parts.
I. In Part one, a review of published material pertaining to
distribution plates, including details from the patent specifications, has
been prepared. After a chapter on the determination of the incipient
fluidizing velocity, the following aspects of multi-orifice distributor
plates in gas fluidized beds have been studied:
(i) The effect of the distributor on bubble formation related to the
way in which even distribution of bubbles on the top surface of the fluidized
bed is obtained, e.g. the desirable pressure drop ratio for
the even distribution of gas across the bed.
Ratios of distributor pressure drop to bed pressure drop at which
stable fluidization occurs show reasonable agreement with industrial
practice. There is evidence that larger diameter beds tend to be less
stable than smaller diameter beds when these are operated with shallow beds.
Experiments show that in the presence of the bed the distributor
pressure drop is reduced relative to the pressure drop without the bed,
and this pressure drop in the former condition is regarded as the appropriate
parameter for the design of the distributor.
(ii) Experimental measurements of bubble distribution at the surface
has been used to indicate maldistribution within the bed. Redistribution
is more likely at low gas flow rates and with distributors having large
fractional free area characteristics (i.e. with distributors having low
pressure drops).
Bubble sizes obtained from this study, as well as those of others,
have been successfully correlated. The correlation produced implies the
existence of a bubble at the surface of an orifice and its growth by the addition of excess gas from the fluidized bed.
(iii) For a given solid system, the amount of defluidized particles
stagnating on the distributor plate is influenced by the orifice spacing,
bed diameter and gas flow rate, but independent of the initial bed height
and the way the orifices are arranged on the distributor plate.
II. In Part two, solids flowback through single and multi-orifice
distributors in two-dimensional and cylindrical beds of solids fluidized
with air has been investigated. Distributors equipped with long cylindrical
nozzles have also been included in the study.
An equation for the prediction of free flowback of solids through
multi-orifice distributors has been derived. Under fluidized conditions two
regimes of flowback have been differentiated, namely dumping and weeping.
Data in the weeping regime have been successfully correlated. The limiting
gas velocity through the distributor orifices at which flowback is
completely excluded is found to be indepnndent of bed height, but a function
of distributor design and physical properties of gas and solid used. A
criterion for the prediction of this velocity has been established.
The decisive advantage of increasing the distributor thickness or
using nozzles to minimize solids flowback in fluidized beds has been
observed and the opportunity taken to explore this poorly studied subject
area. It has been noted, probably for the first time, that with long
nozzles, there exists a critical nozzle length above which uncontrollable
downflow of solids occurs. A theoretical model for predicting the critical
length of a bundle of nozzles in terms of gas velocity through the nozzles
has been set up.
experiments.
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